Characterization of pores in polished low temperature co-fired glass-ceramic composites for optimization of their micromachining

ORCID
0000-0001-7199-7600
Affiliation
Technische Universität Ilmenau , Institute of Micro-and Nanotechnologies MacroNano,Germany
Bartsch, Heike;
ORCID
0000-0002-8020-9458
Affiliation
Alferov University, St. Petersburg,Russia
Lubov, Maksim;
ORCID
0000-0001-8648-4429
Affiliation
Alferov University, St. Petersburg,Russia
Kharlamov, Vladimir;
ORCID
0000-0003-4303-3083
Affiliation
Institute of Research on Electron Microscopy and Materials IMEYMAT, University of Cádiz,Spain
Jiménez, Juan Jesús;
GND
173918050
Affiliation
Institute of Research on Electron Microscopy and Materials IMEYMAT, University of Cádiz,Spain
Morales Sánchez, Francisco Miguel;
ORCID
0000-0002-2611-7720
Affiliation
Technische Universität Ilmenau , Institute of Micro-and Nanotechnologies MacroNano,Germany
Pezoldt, Jörg

Pores are intrinsic defects of ceramic composites and influence their functional properties significantly. Their characterization is therefore a pivotal task in material and process optimization. It is demonstrated that polished section analysis allows for obtaining precise information on pore size, shape, area fraction, and homogeneous distribution. It is proven that laser scanning microscopy provides accurate height maps and is thus an appropriate technique for assessing surface features. Such data is used to compare areas with good and poor polishing results, and various surface parameters are evaluated in terms of their informative value and data processing effort. The material under investigation is a low temperature co-fired ceramic composite. Through statistical analysis of the data, the inclination angle was identified as an appropriate parameter to describe the polishing result. By using masked data, direct conclusions can be drawn about the leveling of load-bearing surface areas, which are crucial in photolithographic processing steps and bonding technology. A broad discussion of different defects based on the results contributes to a critical analysis of the potentials and obstacles of micromachining of low temperature cofired ceramic substrates.

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